Published: Journal of Analytical Toxicology, Volume 21, Number 7, November/December 1997, pp. 576–579.
CASE REPORT: Diltiazem and Pentoxifylline Determination in
Postmortem Specimens
D.A. Engelhart, E.S. Lavins,
S.S. Seligman, and C.A. Sutheimer
A 78-year-old woman was found dead in her basement. Qualitative screening of available postmortem specimens detected the presence of diltiazem and pentoxifylline. Quantitations were carried out by gas chromatography using nitrogen-phosphorus detection and confirmed by gas chromatography–mass spectrometry with the following results: blood, 0.59 mg/dL diltiazem and 0.63 mg/dL pentoxifylline; urine, 1.17 mg/dL diltiazem and 0.08 mg/dL pentoxifylline; bile, 0.40 mg/dL diltiazem and 0.22 mg/dL pentoxifylline; gastric contents, 0.28 mg/dL diltiazem and 0.02 mg/dL pentoxifylline. Both drugs were found qualitatively in formalin-fixed tissues.
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